27 مهر 1398
محمود ناصري

محمود ناصری

مرتبه علمی: دانشیار
نشانی:
تحصیلات: دکترای تخصصی / فیزیک-نانو
تلفن: 08132355404
دانشکده: علوم پایه

مشخصات پژوهش

عنوان
Superparamagnetic magnesium ferrite nanoparticles fabricated by a simple,thermal-treatment method
نوع پژوهش مقاله چاپ شده
کلیدواژه‌ها
Magnetic material Microstructure Nanoparticle Thermal-treatment Polymer
سال
2014
مجله JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS
پژوهشگران محمود ناصری

چکیده

This study investigated the synthesis of magnesium ferrite (MgFe2O4) nanoparticles with cubic symmetry that were prepared by a thermal-treatment method by using a solution that contained poly (vinyl alcohol) (PVA) as a capping agent and Mg and Fe nitrates as alternative sources of metal. Heat treatment was conducted using an electric cylinder furnace in an air atmosphere at temperatures between 673 and 973 K, and magnesium ferrite nanoparticles were produced that had different crystallite sizes ranging from5 to 8 nm. The products were well characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), field emission scanning electron microscope (FESEM), X-ray analysis (EDXA), and Fourier transform infrared spectroscopy (FT-IR). All the samples calcined from 673 to 973 K exhibited super paramagnetic behavior with unpaired electrons spins, which was confirmed by using a vibrating sample magnetometer (VSM) and electron paramagnetic resonance (EPR) spectroscopy.